Influence of Annealing Temperature on the Nanostructural Formation of Ti4Ti5O12 Lithium Battery Anode Material

Renny Nazario-Naveda; Segundo Rojas-Flores; Moises Gallozzo-Cardenas; Luisa Juarez-Cortijo; Daniel Delfin-Narciso; Milton Martinez-Julca

doi:10.1109/CGEE59468.2023.10351826

Influence of Annealing Temperature on the Nanostructural Formation of Ti₄Ti₅O₁₂ Lithium Battery Anode Material

Renny Nazario-Naveda, Segundo Rojas-Flores, Moises Gallozzo-Cardenas, Luisa Juarez-Cortijo, Daniel Delfin-Narciso, Milton Martinez-Julca

Producción científica: Capítulo del libro/informe/acta de congreso › Contribución a la conferencia › revisión exhaustiva

Resumen

In this study, Li₄Ti₅O₁₂ (LTO) was synthesized by the sol-gel method, and the influence of the annealing temperature on the formation of the spinel structure of the material was studied for its use as anode material in lithium batteries. The structures of the synthesized materials were evaluated by X-ray diffraction (XRD), while the morphology, by scanning electron spectroscopy (SEM). LTO nanocrystals with a particle size between 24 and 35 nm joined in highly porous agglomerates were obtained. LTO nanocrystals with TiO₂ impurities in their anatase and rutile phases were obtained at temperatures below 700 °C, diffusing from this temperature and obtaining higher purity LTO nanocrystals in the spinel phase at temperatures above 750 °C. The lattice parameter calculations confirm the successful formation of the material.

Idioma original	Inglés
Título de la publicación alojada	2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023
Editorial	Institute of Electrical and Electronics Engineers Inc.
Páginas	97-100
Número de páginas	4
ISBN (versión digital)	9798350339796
DOI	https://doi.org/10.1109/CGEE59468.2023.10351826
Estado	Publicada - 2023
Publicado de forma externa	Sí
Evento	4th International Conference on Clean and Green Energy Engineering, CGEE 2023 - Ankara, Turquía Duración: 26 ago. 2023 → 28 ago. 2023

Serie de la publicación

Nombre	2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023

Conferencia

Conferencia	4th International Conference on Clean and Green Energy Engineering, CGEE 2023
País/Territorio	Turquía
Ciudad	Ankara
Período	26/08/23 → 28/08/23

ODS de las Naciones Unidas

Este resultado contribuye a los siguientes Objetivos de Desarrollo Sostenible

Acceder al documento

10.1109/CGEE59468.2023.10351826

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Nazario-Naveda, R., Rojas-Flores, S., Gallozzo-Cardenas, M., Juarez-Cortijo, L., Delfin-Narciso, D., & Martinez-Julca, M. (2023). Influence of Annealing Temperature on the Nanostructural Formation of Ti₄Ti₅O₁₂ Lithium Battery Anode Material. En 2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023 (pp. 97-100). (2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023). Institute of Electrical and Electronics Engineers Inc.. https://doi.org/10.1109/CGEE59468.2023.10351826

Nazario-Naveda, Renny ; Rojas-Flores, Segundo ; Gallozzo-Cardenas, Moises et al. / Influence of Annealing Temperature on the Nanostructural Formation of Ti₄Ti₅O₁₂ Lithium Battery Anode Material. 2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023. Institute of Electrical and Electronics Engineers Inc., 2023. pp. 97-100 (2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023).

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title = "Influence of Annealing Temperature on the Nanostructural Formation of Ti4Ti5O12 Lithium Battery Anode Material",

abstract = "In this study, Li4Ti5O12 (LTO) was synthesized by the sol-gel method, and the influence of the annealing temperature on the formation of the spinel structure of the material was studied for its use as anode material in lithium batteries. The structures of the synthesized materials were evaluated by X-ray diffraction (XRD), while the morphology, by scanning electron spectroscopy (SEM). LTO nanocrystals with a particle size between 24 and 35 nm joined in highly porous agglomerates were obtained. LTO nanocrystals with TiO2 impurities in their anatase and rutile phases were obtained at temperatures below 700 °C, diffusing from this temperature and obtaining higher purity LTO nanocrystals in the spinel phase at temperatures above 750 °C. The lattice parameter calculations confirm the successful formation of the material.",

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doi = "10.1109/CGEE59468.2023.10351826",

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Nazario-Naveda, R, Rojas-Flores, S, Gallozzo-Cardenas, M, Juarez-Cortijo, L, Delfin-Narciso, D & Martinez-Julca, M 2023, Influence of Annealing Temperature on the Nanostructural Formation of Ti₄Ti₅O₁₂ Lithium Battery Anode Material. En 2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023. 2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023, Institute of Electrical and Electronics Engineers Inc., pp. 97-100, 4th International Conference on Clean and Green Energy Engineering, CGEE 2023, Ankara, Turquía, 26/08/23. https://doi.org/10.1109/CGEE59468.2023.10351826

Influence of Annealing Temperature on the Nanostructural Formation of Ti₄Ti₅O₁₂ Lithium Battery Anode Material. / Nazario-Naveda, Renny; Rojas-Flores, Segundo; Gallozzo-Cardenas, Moises et al.
2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023. Institute of Electrical and Electronics Engineers Inc., 2023. p. 97-100 (2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023).

Producción científica: Capítulo del libro/informe/acta de congreso › Contribución a la conferencia › revisión exhaustiva

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AU - Nazario-Naveda, Renny

AU - Rojas-Flores, Segundo

AU - Gallozzo-Cardenas, Moises

AU - Juarez-Cortijo, Luisa

AU - Delfin-Narciso, Daniel

AU - Martinez-Julca, Milton

PY - 2023

Y1 - 2023

N2 - In this study, Li4Ti5O12 (LTO) was synthesized by the sol-gel method, and the influence of the annealing temperature on the formation of the spinel structure of the material was studied for its use as anode material in lithium batteries. The structures of the synthesized materials were evaluated by X-ray diffraction (XRD), while the morphology, by scanning electron spectroscopy (SEM). LTO nanocrystals with a particle size between 24 and 35 nm joined in highly porous agglomerates were obtained. LTO nanocrystals with TiO2 impurities in their anatase and rutile phases were obtained at temperatures below 700 °C, diffusing from this temperature and obtaining higher purity LTO nanocrystals in the spinel phase at temperatures above 750 °C. The lattice parameter calculations confirm the successful formation of the material.

AB - In this study, Li4Ti5O12 (LTO) was synthesized by the sol-gel method, and the influence of the annealing temperature on the formation of the spinel structure of the material was studied for its use as anode material in lithium batteries. The structures of the synthesized materials were evaluated by X-ray diffraction (XRD), while the morphology, by scanning electron spectroscopy (SEM). LTO nanocrystals with a particle size between 24 and 35 nm joined in highly porous agglomerates were obtained. LTO nanocrystals with TiO2 impurities in their anatase and rutile phases were obtained at temperatures below 700 °C, diffusing from this temperature and obtaining higher purity LTO nanocrystals in the spinel phase at temperatures above 750 °C. The lattice parameter calculations confirm the successful formation of the material.

KW - anode material

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KW - LTO

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T3 - 2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023

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BT - 2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023

PB - Institute of Electrical and Electronics Engineers Inc.

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Nazario-Naveda R, Rojas-Flores S, Gallozzo-Cardenas M, Juarez-Cortijo L, Delfin-Narciso D, Martinez-Julca M. Influence of Annealing Temperature on the Nanostructural Formation of Ti₄Ti₅O₁₂ Lithium Battery Anode Material. En 2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023. Institute of Electrical and Electronics Engineers Inc. 2023. p. 97-100. (2023 4th International Conference on Clean and Green Energy Engineering, CGEE 2023). doi: 10.1109/CGEE59468.2023.10351826